Unlike volumes 1 and 2, volumes 3 and 4 do not actually have chapter breaks as an aid on the two-episode sides. Volume 4 is the first one not to list included episodes on the sleeve, so without direct inspection, the sketch sampling listed is the only clue to the contents, and episode order can only be determined by direct use.
- Side 1:
- No. 32 (Series 3, Episode 6, 1972)
- No. 24 (Series 2, Episode 11, 1970)
- Side 2:
- No. 33 (Series 3, Episode 7, 1972)
Episode 33 contains the full "Biggles dictates a letter" sketch, which is missing a line or so ("I am not a Spanish person") on the A&E DVD.
Episode 24 is the same as the generally available version and does not include any lost content such as the longer religion animation (or the brief mention of cancer in the opening Conquistador Coffee sketch). It does have the full Crelm toothpaste sketch. (The long-lost black-and-white 16mm version of the episode has the first two but not the third.)
The copyright card for episode 33 is missing, as are company logos (Devillier-Donegan Enterprises and/or Paramount, which end the other volumes). After the episode fades out, all that remains is the LaserVision Side 2 card.